Visuals for Bruker DRX-600 NMR Training Workshop Lecture I

These visuals are made from the original lecture transparencies 

•    The Bruker DRX-600 at U of A CBC
•    Upgrades to the Bruker DRX-600
•    Outline: Advanced 1D Experiments
•    Advanced 1D Experiments
•    Steady-State NOE difference
•    NOE difference: pulse sequence diagram
•    Heat Transfer Analogy
•    Steady-state NOE: heat transfer analogy
•    NOE difference: Sucrose H-g1
•    NOE difference: Cholesterol H4ab
•    Transient NOE
•    Transient NOE: Heat flow analogy
•    Transient NOE: z-magnetization vs time
•    Shaped (Selective) Pulses
•    What is the "excitation profile" of a pulse?
•    Selective Gaussian pulse on Sucrose at Different Frequencies
•    Combining Pulsed Field Gradients and Shaped Pulses
•    Pulsed field gradients - on vs off
•    Effect of a Gradient Pulse on Sample Net Magnetization
•    Gradient Echo: Profile of NMR Tube
•    Effect of 180^o Pulse on Twisted Coherence
•    Gradient-enhanced spin-echo
•    Gradient-enhanced spin-echo: Selected Magnetization
•    Gradient-enhanced spin-echo: Other (non-selected) Magnetization
•    Double Pulsed Field Gradient Spin Echo: A.J. Shaka
•    Selective 1D Transient NOE: A J Shaka
•    500 MHz ¹H spectrum of cholesterol: H4eq and H4ax signals
•    Selective 1D NOE: results for H4eq (top) and H4ax (bottom)
•    Transient NOE buildup curves for Sucrose H-f1 to H-g1 and H-f3
•    1D TOCSY
•    Selective 1D TOCSY: pulse sequence using PFGSE
•    TOCSY 2D vs TOCSY 1D: pulse sequences
•    TOCSY: spin systems and downfield "handles"
•    TOCSY: how far can you go?
•    Results: selecting sucrose H-g1
•    Results: selecting cholesterol H3 (top) and H6 (bottom)
•    Structure Diagram: selecting cholesterol H3
•    Structure Diagram: selecting cholesterol H6
•    Parameters for Selective 1D Experiments on the DRX-600
•    XWinNMR Software
•    General Setup Procedure for DRX-600